Bulk electrolysis of a NE solution using the Ag bed electrode. The potential set point was 0.6 V with the measured potential plotted. The solution composition was 0.8 M NE + 0.85 M NaOH + 1.6 M NaNO2. The solution (10 mL) was continuously pumped from the collection flask back to the top of the cell. After the reaction was complete the cell was rinsed with additional 0.5 M NaOH solution to remove remaining product
A plot of the current and potential versus time for potentiostatic
electrolysis at 0.6 V is shown in Fig. 6 .
The batch electrolysis shown in Fig. 6 , after condensation
with formaldehyde to form DNPOH, yielded 57.6% molar yield and 75%
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